By Aldo Ghizzetti (auth.), Aldo Ghizzetti (eds.)
A. Ghizzetti: a) Lezioni sui procedimenti di quasilinearizzazione e applicazioni. b) Nozioni fondamentali sulle equazioni alle differenze e sulle frazioni continue.- P. Wynn: 4 lectures at the numerical program of endured fractions.- W. Gautschi: power and weak point of three-term recurrence relation.- F.L. Bauer: Use of endured fractions and algorithms on the topic of them.
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Extra resources for Alcune questioni di analisi numerica
II. Description of instrument. . . . a) Gas chromatograph and combustion section b) Titration cells for halide and sulfur . c) Furnace control module d) Coulometer module . e) Recorder and integrator III. Operation of the MCGC . IV. Determination of pesticide residues V. Calculation of results. . VI. Maintenance . . . . a) Care of halide titration cell . b) Care of sulfur titration cell . VII. Discussion of gas chromatography unit a) Chromatographic columns b) Injection block . .
Acetone . . . Ethanol. • . . Diethyl ether. . Methylene chloride Chloroform Benzene Methanol . • Toluene Dichloroethane . 29 26 36 41 53 55 60 61 68 99 182 It is obvious from these results that solvent has a great effect ov \ rescence intensity. In addition, there does not appear to be any L D. MACDoUGALL 32 sequence in the relation of fluorescence intensity to solvent type. It is noteworthy that this acid is least fluorescent in dichloroethane, while chloroform gives an intermediate value.
This condition is detected by malformed peaks and low recoveries afl:er the installation of a new column. The block can be cleaned out by removing it from the oven, washing it with 5 percent alkali, concentrated nitric acid, water, and a final rinse with acetone. J' will! ~mmm --- - - -- - - - 127mm --'---'-------- Srale: I"- 1 // Vycor or 'Iuarlz if/serl lube Fig. 8. Detailed drawing of quartz injection tube and necessary changes in MCGC blod< for use of the tube Pesticide residue analysis by microcoulometric gas chromatography 55 Many plant extracts cannot be injected into the block without contamination to the point of obtaining atypical peaks and recoveries.
Alcune questioni di analisi numerica by Aldo Ghizzetti (auth.), Aldo Ghizzetti (eds.)